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Direct electrochemical extraction of Ti5Si3 from pressed cathode pellets comprising of powdered Ti/Sicontaining metal oxide compounds was investigated by using molten salt electro-deoxidation technology.Three groups of mixtures including TiO2 mixed with SiO2,Ti-bearing blast furnace slag(TBFS) mixed with TiO2, and TBFS mixed with high-titanium slag(HTS) were prepared at the same stoichiometric ratio(Ti:Si=5:3) corresponding to the target composition of Ti5Si3,and used as the starting materials in this experiment,respectively. The pressed porous cylindrical pellet of the Ti/Si-containing compounds served as a cathode,and two different anode systems,i.e.,the inert solid oxide oxygen-ion-conducting membrane(SOM) based anode system and graphite-based anode system were used contrastively.The electrochemical experiment was carried out at 900-1050℃and 3.0-4.0 V in molten CaCl2 electrolyte.The results show that the oxide components were electro-deoxidized effectively and Ti5Si3 could be directly extracted from these complex Ti/Si-containing metal oxide compounds. 相似文献
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结合断面的颤振导数,采用阶跃函数对桥梁断面自激力进行模拟,并对模拟准确性进行了分析与校核;推导出时域颤振动力有限元分析中自激力的递推表达式。基于阶跃函数拟合气动力,利用APDL语言在ANSYS中实现了颤振时域分析;以一简支梁为例,介绍了在ANSYS中实现颤振时程分析的过程。数值算例计算结果和相关文献报道基本一致。研究表明:利用ANSYS的二次开发平台进行桥梁气动稳定性能的时域分析是可行的,该方法可提高桥梁颤振分析或颤抖振理论分析效率,降低自主开发大型软件过程中的算法错误或疏漏所带来的风险。 相似文献
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由于隧道宽度的限制,重型铰接式汽车在隧道中调头不仅费时费力,而且污染工作环境,通过增设新的调头机构可很好地解决定一问题,文章对该机构的设计及操作方法进行了阐述。 相似文献
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