| 离子交换法制备硫酸钙晶须及其表征 |
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| 引用本文： | 王莹,李准,李彦生.离子交换法制备硫酸钙晶须及其表征[J].大连铁道学院学报,2010(2):51-55. |
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| 作者姓名： | 王莹 李准 李彦生 |
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| 作者单位： | 大连交通大学环境与化学工程学院; |
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| 摘 要： | 以离子交换树脂为模板,在20~80℃的温度条件和600 r/min的搅拌作用下,与硫酸盐溶液反应,制备硫酸钙晶须.讨论了不同反应条件包括反应温度、硫酸盐溶液浓度和反应时间对产物的影响,由实验结果可知,40~60℃的温度条件,2~4 h的反应时间,0.17~0.35 mol/L的硫酸锌浓度是最佳制备条件.同时由SEM、TG、XRD和IR分析的结果表明,使用该方法可以得到形貌规整、均一的半水硫酸钙晶须.
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| 关 键 词： | 离子交换 硫酸钙 表征 |
Preparation and Characterization of Calcium Sulfate Whiskers by Ion-Exchange Method |
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| WANG Ying,LI Zhun,LI Yan-sheng.Preparation and Characterization of Calcium Sulfate Whiskers by Ion-Exchange Method[J].Journal of Dalian Railway Institute,2010(2):51-55. |
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| Authors: | WANG Ying LI Zhun LI Yan-sheng |
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| Institution: | WANG Ying,LI Zhun,LI Yan-sheng(School of Environmental & Chemical Engineering,Dalian Jiaotong University,Dalian 116028,China) |
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| Abstract: | Calcium sulfate whiskers are prepared with ion-exchange resins as templates and sulfate solution at 20～80℃ reactive temperature and 600r/min stirring rate.The effects of different reactive conditions including reactive temperature,time and concentration of zinc sulfate solution on products are discussed,which show that the optimal conditions are respectively 40～60℃,4～6h and 0.2～0.35mol/L.The results of SEM,TG,XRD and IR show that the regular and uniform calcium sulfate whiskers can be obtained by the ion-exchange method. |
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| Keywords: | ion exchange calcium sulfate characterization |
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