染毒试片中残留正丙硫醚的反相高效液相色谱法测定

本研究的目的是为了建立染毒试片中残留正丙硫醚的反相高效液相色谱(RP-HPLC)分析方法.本研究方法以ODS-C18柱(250 mm ×4.6 mm)作为色谱分离柱,80%甲醇:20%水(V/V)为流动相,流速为1.0 mL/min,检测波长为205 nm的紫外检测器.结果表明,正丙硫醚在0.3～60 mg/L范围内呈良好的线性关系,检出限为0.18mg/L(S/N=3),添加回收率在92%以上,RSD均在2.0%以下.这表明,RP-HPLC法可应用于染毒试片中残留正丙硫醚的测定.     

Li/SF6热源在鱼雷和UUV推进系统中的应用

基于L i/SF6燃烧反应的特点,简述了其作为热源在鱼雷和无人水下航行器(UUV)推进系统中的应用,论述了热管式反应器为UUV提供动力的特点和优势,并对国外学者有关L i/SF6的毛细反应方面的研究情况作了介绍。     

破片与冲击波对固支方板的耦合毁伤效应数值研究

为探索固支方板在破片与冲击波耦合作用下的典型破坏模式及临界转换条件,采用耦合的SPH-FEM方法数值模拟靶板在破片与冲击波耦合作用下的破坏过程。结果表明:(1)耦合载荷作用下靶板的损伤模式主要分成两种,模式I:花瓣弯曲破坏;模式Ⅱ:拉伸断裂破坏。模式Ⅱ还可细分为两种,模式Ⅱa:板边界产生塑性变形,中心产生拉伸断裂破坏;模式Ⅱb:板边界和中心均产生拉伸断裂破坏。(2)模式I和模式Ⅱa之间的临界i*(无量纲冲量)值约为0.88;模式Ⅱa与模式Ⅱb之间的临界i*值约为0.64。(3)靶板的破口面积并不是随着i*的增大而增大,当i*=0.71时,破口面积达到最大值,约为抗爆有效面积的68%。     

港口吞吐量的随机分析

货船按参数为λ的泊松过程{N(t),t≥0}进入港口,各货船所装卸货物的重量形成一族独立同分布的随机变量{Xi,i=1,2,},在t时间内货船装卸的货物可用Y(t)=∑=N(t)(i=1)Xi表示,其中{N(t),t≥0}和{Xi,i=1,2,}相互独立,这可看作是一个复合泊松过程,并从随机过程的角度分析了港口在t时间内总吞吐量的数字特征,证明货物总吞吐量过程具有独立平稳增量性。     

反相高效液相色谱法测定染毒漆板中马拉硫磷残留量

采用反相高效液相色谱法测定染毒漆板上马拉硫磷残留量。本研究方法以ODS-C18柱（250mm×4.6mm）作为色谱分离柱,80%甲醇：20%水（V/V）为流动相,流速为1.0ml/min,检测波长为220nm的紫外检测器。研究结果表明,在10-100mg/L浓度范围内峰面积与进样量呈良好的线性关系,相关系数r=0.9999;检出限为6.5μg/L（S/N=3）;相对标准偏差RSD为1.36%;平均加标回收率在95%以上。     

消息报道

上海新中动力机厂引进西德 M.A.N 公司专利生产的新中——M.A.N.L20/27中速柴油机巳在沪制造成功;并经中国船舶检验局和英国劳氏船级社检验认可。该机分 L 型,(4,5,6,7,8,9缸);V 型(12,14,16,18缸);转速有:1000,900,750,720转/分四种;功率从288千瓦(392马力)至1800千瓦(2448马力);可燃用轻柴油或雷氏2100     

固相萃取-气相色谱法测定水中有机氯农药

建立了固相萃取(SPE)-气相色谱/电子捕获检测器(GC/ECD)同时测定水中20种有机氯农药的方法,并对固相萃取条件进行了优化.实验表明,该方法具有较好的线性关系(相关系数为0.997 0～0.999 8),对于1 L添加0.5 μg有机氯农药混合标准溶液水样,其目标化合物的回收率为64.1%～123.2%,检出限为0.001～0.01μg/L,多次重复实验测定的相对标准偏差小于15%(n=6).     

简析伟大联盟和新世界联盟的合作

1两个联盟宣布合作2005年10月6日,伟大联盟(the G rand A l-liance——G A)和新世界联盟(The N ew W orld A l-liance——TN W A)各成员(除PO N L)同时对外宣布,两个联盟(不包括PO N L)将从2006年开始,在主干航线上开始合作。双方将首先在亚洲——欧洲航线上开展舱位互换并开辟     

离子色谱法测定潜艇舱室气体中无机阴离子研究

研究了电导检测器-离子色谱同时测定潜艇舱室气体中的F-,Cl-,NO2-,NO3-,SO42-等五种无机阴离子分析方法.使用Shim-pack IC-A2(5.0mmφ×5cm)离子色谱柱,以0.75mmol/L邻苯二甲酸氢钾(PH 4.2)为淋洗液,流速为1.0mL/min,可以较好地将五种阴离子进行分离,其中F-的测定相对标准偏差(RSD)为1.4%～5.9%.     

高强度钛青铜热处理工艺及组织性能研究

为了替代污染严重和价格昂贵的CuCo2Be,文中介绍了合金元素总量小于3.5%的钛青铜,确定了其最佳热处理和冷变形工艺,在900℃×1h(水淬) 20%(冷变形) 510℃×1.5h(时效)的典型工艺条件下,其综合性能达到了标准规定的CuCo2Be合金水平。并对钛青铜不同工艺条件下的金相组织及室温和高温断口进行了观察、分析,利用TEM研究了合金的微观结构,结果表明该合金属于N i3Ti和Cr的复合沉淀强化,主要析出相N i3Ti弥散分布于基体,颗粒尺寸在20 nm左右。与CuCo2Be相比,钛青铜的晶粒度对温度变化较为敏感,故应避免在过时效状态下使用。     

Errata

正In the paper"Influence of Fouling Assemblage on the Corrosion Behaviour of Mild Steel in the Coastal Waters of The Gulf of Mannar,India"in Vol.12,No.4,Page:509,References were lost,and the two authors’biographies were identical.The correct text is shown below.We apologize to the authors and our readers for any inconvenience caused by the errors.     

Journal of Marine Science and Application 2014 Sum. Contents

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第34届海洋、离岸及极地工程国际会议(英文)

正St.John's,Newfoundland,Canada,May 31-June 5,2015 OMAE2015 is the ideal forum for researchers,engineers,managers,technicians and students from the scientific and industrial communities from around the world to: meet and present advances in technology and its scientific support;     

联合作战计划和执行系统

全球指挥控制系统(GCCS)实施当前美国海军网络中心战信息基础设施的联合计划网络。联合作战计划和执行系统(JOPES)支持GCCS实现联合计划。JOPES有两类计划：时间不限的精密预案计划生成作战计划、方案计划或职能计划；时间敏感的危机行动计划生成作战命令或战役方案。前者在和平时期创建的作战计划是后者的计划基础，加速应付危机的能力。     

Eastbound or westbound ?

In terms of equal sailing distances, where is the inflexion when ships depart from ports in the Asian Continent to New York via Suez and/or Panama？
The answer is China South Port Group （Hong Kong, Shenzhen and Guangzhou）.     

Recent progress on wave induced loading measurements in warships

Recent measurements of wave induced hull strain and flexure in RN warships are presented together with the derivation of the current design criteria for extreme hull girder bending loads. The history of the development of the shipboard instrumentation used is given and recent developments to improve the quality and ease of analysis of the data are described. An unexpectedly high transverse asymmetry in the longitudinal strains measured in destroyers is shown to be the result of a combination of vertical and lateral bending in oblique seas. Finally recent theoretical comparisons between the loading of Deep-Vee hulls and conventional UK rounded bilge hulls are presented which demonstrate the higher loading experienced by this type of hull form.     

桥梁防撞设施物理模型试验

物理模型试验是预报防撞设施所受撞击力及优化设计方案的主要方法之一。结合杭州湾大桥柔性防撞设施及东海大桥独立式防撞体设计方案,阐述了船—防撞体撞击试验的基本原理、方法、试验方案及相关试验结果。提出了柔性防撞系统的优化方案。试验结果表明,该方案经济有效,可供预报类似桥梁防撞设施撞击力时参考。     

印尼某电厂码头水工建筑物设计

印尼某电厂项目码头水工建筑物包括码头、防波堤和护岸等主要组成部分。在该项目水工建筑物的设计过程中,综合考虑当地的自然条件、施工能力和材料来源等因素,不断优化结构选型和结构断面。根据不同使用要求,护岸分别采用直立式和斜坡式2种结构型式,推荐的设计方案节省投资、施工方便,可供同类工程设计参考。     

Impact of regulation on the performances of long-distance transport services: A comparison of the different approaches in Sweden and Norway

Despite the many socio-economic similarities between Sweden and Norway, differences in jurisdiction, organisation, cooperation, and financing of long-distance passenger train and coach services have led to the development of four distinctively different ways of serving the markets. This paper describes how the train and coach markets have developed in the two countries, with emphasis on regulatory and industrial structure and a couple of performance variables.Looking at passenger rail, both countries separated infrastructure from operation over a decade ago. However, while Norwegian rail is characterised by an almost monopoly supplier, rail services in Sweden are partly decentralised to the responsibility of county authorities and are widely subjected to competitive tendering. The rest of the network is about to be opened up for on-the-track competition. Swedish Rail (SJ) has spent the last decades consolidating its core business (passenger rail) and sold out its other businesses. In contrast, the Norwegian state rail (NSB) has expanded its business to become a major bus operator and property owner, with extensions also into the Swedish market.The coach industry was more recently deregulated in both countries. The Swedish coach market is dominated by privately owned companies operating services to and from Stockholm. In Norway, state-owned NSB is a major coach operator on medium distance routes, and is also the largest partner of Nor-Way Bussekspress which totally dominates long-distance coach services. Further, the Norwegian coach market is characterised by cross-ownership and cooperation which has enabled an extensive route network which covers most of Norway.We find distinct differences in achievements in the two modes and in the two countries. Swedish rail services have succeeded in winning market shares and in renewing and developing both infrastructure and service levels to a greater extent than the Norwegian model. On the other hand, the Norwegian coach market seems to be more developed and efficient compared to its Swedish counterpart.The paper concludes with a discussion on the possible links between the different approaches and the performance observed, with the aim to stimulate further and more detailed research on some important issues.     

开放式数据挖掘系统模型

目前国内已经出现了少量的数据挖掘相关产品。国内数据挖掘软件无论从数量还是质量上比较，都与国外软件存在着较大的差距。随着数据仓库技术的普及，数据挖掘应用的需求越来越强烈，如何缩短这种差距，研发数据挖掘软件产品成为国内业界的一个重要问题。通过引用目前国际通用数据挖掘标准技术来构建开放式的数据挖掘系统模型，该系统模型从可扩展性、可重用性、易用性等方面得到了加强。