铑催化剂用水合三氯化铑的制备

水合三氯化铑是制备铑催化剂的关键原材料之一。随着化工及汽车行业的发展,对铑催化剂有了更多的需求,由此对水合三氯化铑的需求量越来越大。本文综述了当前铑催化剂的应用,以及其原材料水合三氯化铑制备技术的研究进展,并且展望了未来水合三氯化铑的制备技术。     

“三图四表”管理制度在轨交基坑施工中的应用

结合宁波轨交1号线一期工程TJ-Ⅷ标东环南路站工程,参建单位对基坑结构风险进行了静态分析与评估,并对基坑设计方案进行了优化。在基坑开挖过程中,通过"三图四表"管理制度对基坑开挖过程进行动态实时的控制,采取了一系列针对基坑变形的控制措施,顺利完成了该站主体基坑的开挖作业。可供欠固结土地区深基坑的设计和施工参考。     

Automatic outer surface extraction of femoral head in CT images

Computer-aided hip surgery planning and implant design applications require accurate segmentation of femoral head and proximal acetabulum. An accurate outer surface extraction of femoral head using marching cubes algorithm remains challenging due to deformed shapes and extremely narrow inter-bone regions. In this paper, we present an automatic and fast approach for segmentation of femoral head and proximal acetabulum which leads to accurate and compact representation of femoral head using marching cubes algorithm. At first, valley-emphasized images are constructed from original images so that valleys stand out in high relief. Otsu’s multiple thresholding technique is applied to seperate the images into bone and non-bone classes. Region growing method and threedimensional (3D) morphological operations are performed to fill holes in the bone. In the reclassification process, the bone regions are further segmented, and the boundaries of the bone regions are further refined based on Bayes decision rule. Finally, marching cubes algorithm is applied to reconstruct a 3D model and extract the outer surface of femoral head and proximal acetabulum. Experimental results show that this method is an accurate segmentation technique for femoral head and proximal acetabulum and it can be applied as a tool in medical practice.     

基于一维-三维耦合仿真的进气系统优化方法

提出了基于一维-三维耦合仿真的进气系统优化方法,此方法兼具CFD对进气系统三维流动特性准确描述与一维仿真对内燃机进气系统全局控制的优点。建立了进气歧管三维模型,采用GT-Power软件进行缸内工作过程模型仿真,根据试验数据标定仿真模型。通过一维-三维耦合仿真计算得到进气歧管各转速下的流动参数,以此作为CFD仿真的边界条件,优化进气歧管的结构参数。通过整机试验对进气歧管流动性能进行了验证。试验结果表明,该方法能够较好地指导进气歧管设计。     

Flow Stress Model of Stainless Steel OCr13Ni5Mo at Elevated Temperature

For a more accurate forming calculation and numerical simulation of hydraulic turbine blade,experimental studies on the flow stress of stainless steel OCr13Ni5Mo were carried out upon Gleeble-1500 thermal simulator under different deformation conditions.The results then were analyzed and the effects of all influencing factors were summarized consequently.New mathematic models were conceived.Utilizing the software Matlab,regression coefficients were calculated by the least square method.The model has an eminent capability of curve-fitting performance with impact structure whose correlation coefficient is up to 0.908 0 and the cosine coefficient is 0.995 8.All mathematic models and process parameters can be used in engineering calculations or computer simulations.     

新型公路隧道降噪吸音砂浆的制备工艺

文章根据公路隧道对降噪吸音材料的特殊要求,以水泥、陶砂、膨胀珍珠岩等材料为主要原料,结合一系列的拌制工艺,研制出一种环保无污染、防火、防撞击、施工方便快捷、喷覆式的新型隧道吸音材料--陶砂膨胀珍珠岩吸音砂浆,并采用驻波管法测试砂浆的吸音性能.     

城市老城区健康道路交通模式探讨

为解决城市老城区交通压力持续增大的问题,从道路系统、公共交通系统、慢行交通系统三个方面进行研究,基于健康城市理念,并借鉴国外城市老城区交通发展模式,提出国内城市老城区健康道路交通模式应具有道路网络"高密度、小街区、微循环",公共交通全覆盖、高效率,慢行交通空间连续、设施完善、与公共交通无缝衔接等特征,为老城区健康道路交通规划设计提供参考。     

一氧化氮合酶在胃食管反流病患者食道黏膜的表达

目的比较胃食管反流病(GERD)患者与健康对照者食管黏膜中一氧化氮合酶两种亚型(nNOS和iNOS)的表达情况。方法通过免疫组化法检测nNOS和iNOS在食管黏膜的分布和相对的蛋白定量,荧光定量PCR法检测其mRNA的含量。结果 nNOS和iNOS蛋白主要在食管黏膜上皮细胞胞质中表达,反流性食管炎(RE)患者明显高于非糜烂性反流病(NERD)和健康对照组(P<0.05),RE患者nNOS和iNOS的mRNA含量也明显高于NERD患者和健康对照组(P<0.05)。结论反流性食管炎患者食管黏膜中的nNOS、iNOS蛋白和mRNA含量增高,可能是一氧化氮参与胃食管反流病发生的分子机制之一。     

灌河口水动力条件对口门整治工程响应分析

为研究灌河口各整治工程实施后对河口纳潮量、潮位、流速的影响并提出最优的灌河口整治方案,首先分析了灌河口的自然条件;然后构建二维水流数学模型,根据实测资料对模型进行验证;最后利用数学模型对各整治方案实施前后的水力特性变化进行分析。口门整治工程实施后结果表明:仅导堤工程的实施对河口纳潮量影响较大,应配合航道疏浚工程来缓解其带来的影响;导堤工程和航道工程同时实施后,双导堤内水流进一步归顺,流速有所增大,对维持航道水深较有利。     

基于改进TRL校准算法的二极管参数测量

加载二极管的频率选择表面和能量选择表面(以下统称"自激励表面")具有自适应的防护特征,能够防护强电磁攻击。二极管本身参数的测量是自激励表面设计中重要的环节,准确测得二极管特征参数对于设计出满足需求的防护表面至关重要。介绍传统去嵌入法,针对传统去嵌入法存在校准件制作精度要求高、相位延时有范围的缺点,改进了用于二极管参数测量的去嵌入算法;测量几种不同PIN型号的二极管,通过对比PIN参数手册与测试结果,验证了测试方法的有效性。