A rapid method for the determination of dopamine in porcine muscle by pre-column derivatization and HPLC with fluorescence detection

A rapid method has been developed based on the sample preparation procedure named as QuEChERS （Quick, Easy, Cheap, Effective, Rugged and Safe）, combined with reversed-phase high performance liquid chromatography with fluorescence detector and C18 column after precolumn derivatization using o-phthalaldehyde and 2-mercaptoethanol to determine dopamine in porcine muscle. Methanol and deionized water （0.1% acetic acid, v/v） with a ratio of 60：40 was used as mobile phase. The flow rate was 0.8 mL/min and dopamine was eluted within 15 min. The linearity range was 0.003-8 μg/mL with r=0.9992. The detection limit for dopamine was 4 μg/kg and the quantification limit was 9 μg/kg. Recovery studies were carried out at 0.1, 0.5 and 1.0 mg/kg fortification levels and the average recoveries obtained ranged from 90.4% to 98.2% with relative standard deviations between 3.5% and 8.1%. The method was found to be suitable for detection of dopamine in animal product tissues at the maximum residue level.     

THE PROSPECTIVE STUDY OF RELATIONSHIP BETWEEN LOW SELENIUM AND KASHIN-BECK DISEASE

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侧风下车体横向振动对倾覆影响的基础研究

RTRI详细方程式是对侧风下铁道车辆倾覆进行静态分析的一种方法,它用静力替代车体的惯性振动力.然而,由于车体的横向振动是一种动态现象,横向振动对倾覆的影响很可能取决于振动振幅和振动频率.为此,用数值模拟检测了横向振动与轮载变化之间的关系.通过将其与线路运行试验所得数据相比,验证了模拟结果的有效性.     

Pragmatic Turn of National Higher Education and Analysis of Guiding Rules

Nowadays more universities and colleges have taken the cultivation of pragmatic studenet as the core of guiding teaching ide- ology which focuses the task of teaching students practical to meet the demand of society for better employment This trend has to be carried out by the delicate design of teaching schemes and great change of teaching method and students achievement evaluation system.     

采用低压废气再循环改善轿车柴油机燃油经济性及瞬态控制

柴油机是客、货牵引车的最重要动力源。从全球温室效应的影响看,降低柴油机排放的任务十分紧迫。随着对日益增加的氮氧化物(NO_x)、颗粒(PM)和二氧化碳排放的关注,提出了严格的排放法规。未来的排放法规要求采用先进的排放控制技术,如选择性催化还原、稀氮氧化物捕集器和废气再循环技术。废气再循环被广泛用于降低排放。用一种低压废气再循环技术降低轿车柴油机排放,改善发动机的燃油经济性。对1台排量为7 L、装备有低压废气再循环系统的轿车柴油机开展了试验研究。在稳态和瞬态运行工况下,使用低压废气再循环系统比使用常规高压废气再循环系统更能获得改进燃油耗的效果。在发动机处于中速、中等负荷时,使用低压废气再循环系统可降低燃油耗,而NO_x和PM排放并不受影响。     

Hyundai-Kia公司新型2.0L和2.2L4缸柴油机系列

2.2 L柴油机是Hyundai-Kia公司新R系列中第1款满足欧5排放标准的机型,该机以66kw/L和200(N·m)/L达到了单级增压柴油机比功率和比扭矩的最高值,使其动力总成在达到低噪声和低燃油耗的同时具有运动车型的行驶功率,并被批量搭载于Kia Sorento轿车和Hyundai SantaFe轿车.     

DEVELOPMENT OF NEW TYPE OF HAZARDLESS FLUXES USED IN THE MELTING OF Mg-ALLOYS

lIntroductionMagnesium,oneofthelighteststructurematerials,hasbeenwidelyappliedinaviation,machineryandautomobilemanufacturing.Withstrongaffinitytooxygenandporosityofitsoxidefilm,magnesiumisapttoreactwithoxy-gen.Thus,duringthemeltofmagnesiumalloys,specialfluxeshavetobeusedtocoverthemelttokeepitfromfurtheroxidizationorevencom-bustionathightemperature,andtorefineandtodegasitandtoremovethedrossfromthemelt[1j.Thewidelyusedfluxesaremainlycomposedofwaterlesscarnallite(MgCl,-KCl)andsomefluoridesandch…     

AN EXPERIMENTAL STUDY ON UVEOSCLERAL OUTFLOW WITH FITC-BSA AS A TRACER IN RABBIT EYE

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基于PFV策略的连续型元胞自动机交通流模型

科学合理的微观交通流仿真模型是研究交通控制手段有效性的关键.本文结合一种考虑驾驶员视野内前后多车影响的跟驰策略，建立了连续型元胞自动机交通流模型.仿真实验表明，仿真数据与实测数据有较好的拟合性，仿真得到的 K-Q、K-V和 Q-V图能较好地反映实际道路交通流的失稳现象，所建立的模型具有适应不同场景的兼容性与灵活性，能够作为研究我国实际道路交通流问题的仿真工具.     

中国继续充当世界经济引擎?

在开始于1978年、长达25年的经济体制改革中,中国年均经济增长率达到9%的同时,其能源消耗也增长了三倍.直到2003年,中国的这种增长趋势对国际商品市场的影响才变得意义重大,影响范围涵盖了包括从铁矿石到燃煤、从大豆到原油在内的众多原材料市场.