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931.
932.
提出了用电感耦合等离子体原子发射光谱(ICP-AES)法测定高纯六氟化钨中铬、锰、铁、钴、镍、铜、锌、镁、钙、钠、钾、铅及钼等金属元素的含量。六氟化钨极易与空气中的水分发生反应,为此设计了一套与空气隔离的密闭取样系统。在装有待测金属元素的取样器内,先后加入氨水、硝酸、氢氟酸使其溶解并定容,作为ICP-AES分析的待测溶液。在优化的实验条件下,得出各元素的检出限小于0.005mgL-1,方法的回收率在90.5%~104.2%之间,测定值的相对标准偏差(n=11)在3.2%~7.8%之间。最终试验分析结果表明,样品满足高纯六氟化钨技术指标的要求。 相似文献
933.
采用王水湿式消化处理样品,建立了ICP-AES法同时测定霍加拉特剂中Mn、Cu、Na、Al、Ca、Mg和Fe等7种金属元素的方法。通过谱线选择、条件优化和基体匹配等方法消除元素间干扰和基体效应,探讨了酸类型及酸度值对谱线强度的影响,研究了溶液浓度对精密度及线性相关系数的影响。方法的线性相关系数均大于0.999,Mn、Cu、Na、Al、Ca、Mg和Fe的最佳谱线分别为Mn257.610nm、Cu327.393nm、Na589.592nm、Al396.153nm、Ca317.933nm、Mg285.213nm、Fe238.204nm,相应的检出限分别为0.0008、0.0009、0.012、0.028、0.010、0.001、0.004μg/mL,对应测定值的相对标准偏差分别为0.34%、0.87%、0.87%、0.54%、0.48%、0.84%、0.55%,加标回收率为94.2%~104.4%。该方法简便、快捷、准确,可在测定其他催化剂中金属含量时推广应用。 相似文献
934.
935.
Michael G.H. Bell Xin Liu Panagiotis Angeloudis Achille Fonzone Solmaz Haji Hosseinloo 《Transportation Research Part B: Methodological》2011,45(8):1152-1161
This paper transfers the classic frequency-based transit assignment method of Spiess and Florian to containers demonstrating its promise as the basis for a global maritime container assignment model. In this model, containers are carried by shipping lines operating strings (or port rotations) with given service frequencies. An origin–destination matrix of full containers is assigned to these strings to minimize sailing time plus container dwell time at the origin port and any intermediate transhipment ports. This necessitated two significant model extensions. The first involves the repositioning of empty containers so that a net outflow of full containers from any port is balanced by a net inflow of empty containers, and vice versa. As with full containers, empty containers are repositioned to minimize the sum of sailing and dwell time, with a facility to discount the dwell time of empty containers in recognition of the absence of inventory. The second involves the inclusion of an upper limit to the maximum number of container moves per unit time at any port. The dual variable for this constraint provides a shadow price, or surcharge, for loading or unloading a container at a congested port. Insight into the interpretation of the dual variables is given by proposition and proof. Model behaviour is illustrated by a simple numerical example. The paper concludes by considering the next steps toward realising a container assignment model that can, amongst other things, support the assessment of supply chain vulnerability to maritime disruptions. 相似文献
936.
介绍了湘桂铁路客专横寨特大桥斜岩、岩溶地质钻孔桩施工工艺,重点阐述了钻孔桩施工中出现溶洞、斜岩、地表塌陷等特殊情况的处理方法。 相似文献
937.
Xinkai WuHenry X. Liu 《Transportation Research Part B: Methodological》2011,45(10):1768-1786
In this paper a new traffic flow model for congested arterial networks, named shockwave profile model (SPM), is presented. Taking advantage of the fact that traffic states within a congested link can be simplified as free-flow, saturated, and jammed conditions, SPM simulates traffic dynamics by analytically deriving the trajectories of four major shockwaves: queuing, discharge, departure, and compression waves. Unlike conventional macroscopic models, in which space is often discretized into small cells for numerical solutions, SPM treats each homogeneous road segment with constant capacity as a section; and the queuing dynamics within each section are described by tracing the shockwave fronts. SPM is particularly suitable for simulating traffic flow on congested signalized arterials especially with queue spillover problems, where the steady-state periodic pattern of queue build-up and dissipation process may break down. Depending on when and where spillover occurs along a signalized arterial, a large number of queuing patterns may be possible. Therefore it becomes difficult to apply the conventional approach directly to track shockwave fronts. To overcome this difficulty, a novel approach is proposed as part of the SPM, in which queue spillover is treated as either extending a red phase or creating new smaller cycles, so that the analytical solutions for tracing the shockwave fronts can be easily applied. Since only the essential features of arterial traffic flow, i.e., queue build-up and dissipation, are considered, SPM significantly reduces the computational load and improves the numerical efficiency. We further validated SPM using real-world traffic signal data collected from a major arterial in the Twin Cities. The results clearly demonstrate the effectiveness and accuracy of the model. We expect that in the future this model can be applied in a number of real-time applications such as arterial performance prediction and signal optimization. 相似文献
938.
939.
Ronghui Liu Tony May Simon Shepherd 《Transportation Research Part A: Policy and Practice》2011,45(9):951-965
Macroscopic fundamental diagrams (MFD) of traffic for some networks have been shown to have similar shape to those for single links. They have erroneously been used to help estimate the level of travel in congested networks. We argue that supply curves, which track vehicles in their passage through congested networks, are needed for this purpose, and that they differ from the performance curves generated from MFD. We use a microsimulation model, DRACULA and two networks, one synthesizing the network for Cambridge, England, and one of the city of York, England, to explore the nature of performance curves and supply curves under differing patterns of demand.We show that supply curves differ from performance curves once the onset of congestion is reached, and that the incorrect use of performance curves to estimate demand can thus seriously underestimate traffic levels, the costs of congestion, and the value of congestion relief measures. We also show that network aggregated supply curves are sensitive to the temporal distribution of demand and, potentially, to the spatial distribution of demand. The shape of the supply curve also differs between origin–destination movements within a given network.We argue that supply curves for higher levels of demand cannot be observed in normal traffic conditions, and specify ways in which they can be determined from microsimulation and, potentially, by extrapolating observed data. We discuss the implications of these findings for conventional modelling of network management policies, and for these policies themselves. 相似文献
940.