西安地区正常生育力男子的精浆微量元素研究

本文采用原子吸收分光光度法测定了30例有生育力的健康男子精浆中锌、铜、硒、锰、铁、镉、钙及镁8种元素的含量,首次提出了这些元素在精浆中含量的正常估计值范围。精浆中锌、镁及钙之间正相关非常显著,可根据回归方程由三者中的任何1个推算出其它两个的含量。锌及镁还分别与铜正相关,铜与铁负相关。镁含量与精液 pH 负相关,其它元素与精液质量无明显关系。     

体外循环期间血浆与红细胞内钾的改变及补钾方法探索

作者观察了30例心内直视手术患者于体外循环前、中、后血浆钾及红细胞内钾的变化及其影响因素,并分析钾的补充量,发现:灌注前、中的低血钾倾向主要是由于钾向红细胞内转移,而在灌注后主要是尿钾排泄所致;钾的内转移主要受低温、灌注时间及血pH的影响;转流中血钾在4.0m mol/L以下时可导致细胞内钾丢失,提出灌注中补钾量应至少>1.56m mol/kg才能维持血钾在4.0 m mol/L以上。     

表面热处理技术的研究动向

文章从氮化、软氮化、渗碳、碳氮共渗、高频淬火、扩散渗镀、PVD、CVD处理等方面,介绍了当今在这类表面热处理方面的研究动向及取得的新成果,较为详细地评价了上述热处理技术研究中采用的最新试验方法及其实际应用效果,也展现了表面热处理研究的生机活力及发展前景。     

奥氏体不锈钢固溶渗氮研究

对304和904L两种奥氏体不锈钢进行了固溶渗氮研究．用电子探针测定了渗氮层的氮浓度分布，用扫描电子显微镜观察了试样渗层的显微组织，用显微硬度计测量了表面至心部的显微硬度，用X射线衍射仪分析了渗氮层的物相组成，对试样在1mol／L的稀硫酸溶液中的耐蚀性进行了阳极极化曲线分析．结果表明：显微硬度随表面至心部距离的增加而降低．固溶渗氮水冷试样表面的物相为单相奥氏体，炉冷试样的表面物相除高氮奥氏体外，还出现了CrN．渗氮后的试样在1mol／L稀硫酸溶液中的耐蚀性优于未氮化试样．     

Determination of wholesome elements and heavy metals in safflower （Carthamus tinctorius I.. ） from Xinjiang and Henan by

An inductively coupled plasma mass spectrometry （ICP-MS） or inductively coupled plasma atomic emission spectrometry （ICP-AES） was developed to determine 19 elements in safflower, a traditional Chinese medicinal herb from Xinjiang Autonomous Region and Hen     

Rapid quantification of the metabolite of valacyclovir hydrochloride in human plasma by liquid chromatography-tandem mass spectrometry

Objective To establish a rapid, sensitive and selective liquid chromatography-tandem mass spectrometry (LC-MS/MS) method for the determination of acyclovir (the metabolite of valacyclovir hydrochloride) in human plasma. Methods After addition of ganciclovir as internal standard (IS), plasma samples were prepared by one-step protein precipitation using acetonitrile as precipitant, followed by an isocratic elution with 0.1% formic acid 3.5μm) column. Detection was performed on a triple-quadrupole mass spectrometer utilizing electrospray ionization (ESI) interface operating in positive ion and selected reaction monitoring (SRM) mode with the precursor to product ion transitions m/z 226.2→152.1 for acyclovir and m/z 256.2→152.1 for the IS. Results The analytical results demonstrated a good linearity over the ranges from 0.005 to 4μg/mL (r=0.9999) for valacyclovir hydrochloride. The relative standard deviations (RSD) of intra-batch and inter-batch were less than 4.06% and 9.23%, respectively. The limit of detection and lower limit of quantification in human plasma were 2ng/mL and 5ng/mL, respectively. Conclusion The method was simple, sensitive, accurate and reproducible and has been successfully applied to a bioequivalence study of valacyclovir hydrochloride capsules in Chinese healthy male volunteers.     

Analysis of Numerical Results in High Temperature Congealment and Chemistry Non-equilibrium Flow Field

Using the air plasma ignition technique, physicochemical process of burning can be accelerated; concentration limit ofretrofires both can be extended; reliability of retrofires and stability of burning can be improved. In this paper, using internalequivalent heat area in place of electric are that created Ohm heat, the flow fields of thermodynamic equilibrium chemistry con-gealment and chemistry non-equilibrium in the plasma generator were simulated. The influences of the inlet prerotation angleof air, the inlet total pressure of air and the airflow compression angle of spray nozzle on the temperature on the surface of elec-     

结晶器CuNiCoBe合金表面等离子喷涂WC-Co及Mo/WC-Co复合涂层的性能

采用等离子喷涂方法在CuNiCoBe合金表面制备了单一WC-Co涂层和Mo/WC-Co复合涂层.利用扫描电镜(SEM)对涂层的微观形貌进行观察分析,并对涂层的结合强度、抗热震性能以及涂层的摩擦性能分别进行了研究.结果表明:涂层为典型的层叠结构,涂层与基体、涂层与涂层之间结合良好;复合涂层与基体间的结合强度及涂层的抗热震性能均优于单一涂层;WC-Co涂层的平均摩擦系数随着温度的升高而下降.     

氢氧非平衡等离子体法直接合成过氧化氢

在常温常压下,利用介质阻挡放电反应器,通过氢气和氧气的气相等离子体反应直接合成出过氧化氢.考察了反应器结构对过氧化氢合成的影响.结果表明.反应器结构是过氧化氢合成的重要影响参数.在优化条件下,用氢氧等离子体气相反应可获得54%的过氧化氢收率和61%的过氧化氢选择性.     

内燃机微波点火研究进展综述

综述了国内外运用于内燃机的微波点火的研究现状和技术特点,将微波点火主要分为3类,即微波谐振炬点火(Microwave resonator Torch Ignition,MTI)、微波辐射空间点火(Microwave radiation Space Ignition,MSI)、微波等离子体助燃(Microwave plasma Assisted Ignition,MAI),并介绍了微波点火可能的着火燃烧机制。指出微波点火有可能大幅拓展发动机稀燃极限,相对传统火花点火有显著的节能和减排潜力。