具有液晶相的四烷氧基苯并菲-1,4-二醌的合成

研究合成了 6,7,10,11-四戊氧基苯并菲-1,4-二醌和 6,7,10,11-四庚氧基苯并菲-1,4- 二醌两个新化合物,经核磁氢谱和碳谱、质谱、IR 及元素分析等测定,对其结构进行了表征。该类化合物在紫外可见光区 250～630 nm 的范围有光吸收。采用偏光显微镜和示差扫描量热仪对其性能进行了研究,结果表明,该材料具有液晶性。此外,本文对该类化合物的合成方法也进行了改进,利用亚硝酸钠/三氟乙酸/二氯甲烷体系替代了常用的硝酸铈铵/四氢呋喃/水体系,反应时间可从原来的 2 h 缩短至 15 min,并在室温下完成;在合成中间体 1,2-二甲氧基-6,7,10,11-四烷氧基苯并菲时,采用二氯甲烷作为溶剂,将三氯化铁与 3,3＇,4,4＇-四烷氧基联苯的摩尔比从 8∶ 1 提高到 10∶1,反应时间可从原来的 5 h 缩短至 2 h。     

一种船舶柴油机瞬时转速监测记录仪

提出一种基于光电编码器的柴油机抗振动瞬时转速的测量方法,并研制以32位嵌入式处理器(LPC2114)为控制器的瞬时转速监测记录仪。该记录仪分为两级,下位机实时测量柴油机的瞬时转速并发送到上位机,上位机接收数据并进行储存、显示和运算等处理,可进一步得出平均指示压力、缸内燃烧压力等指标,为应用瞬时转速实时评估柴油机的工作状态和故障诊断打下基础。     

Modbus协议在直流牵引供电系统中的应用

以直流牵引供电系统为例,提出了一种基于Modbus协议的通讯方式实现其内部通信。通过对直流牵引供电系统内部通信数据进行分析,采用RS485接口,运用Modbus协议实现了监控软件对微机保护装置和S7-200的串行通信,可靠地实现了系统内部各模块之间的通信,提高了系统的整体运行效率及可靠性。     

7m长发动机后置独立后悬客车底盘

介绍一种全新的7m长发动机后置客车底盘及其主要配置、结构和性能参数等。该底盘采用独立悬架断开式驱动桥,解决了中型客车发动机后置困难、振动噪声大等问题。     

汽车VFD数字显示组合仪表设计

介绍汽车数字显示组合仪表的VFD显示方式和硬件电路的设计原理,对实现该仪表功能的软件方案进行论述。     

国内外铁道机车车辆车轴标准实施

以依据AAR M-101:2013《机车车轴技术条件》生产车轴为例,从及时准确地提供国内外标准及相关信息、提升标准的执行力度和建设技术标准信息平台等3个方面,介绍公司对国内外标准的实施经验。重点从加强标准化宣传与培训工作,改进宣贯模式、提高贯标效果,加强标准执行情况的监督等方面,阐述企业强化标准实施效果的具体做法。     

应用PCR方法检测人乳头瘤病毒的E_7转化基因

应用聚合酶链反应技术（ＰＣＲ）检测５４份子宫颈癌活检标本中人乳头瘤病毒１６型（ＨＰＶ－１６）Ｅ７转化基因的存在情况，结果显示阳性率为７２．２％（３９／５４）。ＨＰＶ－１６Ｅ７转化基因在人子宫颈癌组织中的高检出率，证实该转化基因与其发生关系密切。本研究同时证明，ＰＣＲ方法具有敏感、特异、快速和实用特点，值得推广。     

中欧软质岩灌注桩竖向承载力设计对比

依托某阿布扎比项目,采用欧标和中国规范计算灌注桩竖向承载力,并分析计算结果,对比两个规范的差异性,寻求桩长的合理优化取值。最后,通过现场桩基检测结果对软质岩地质中灌注桩竖向承载力的设计进行验证。研究成果可为类似地质条件下的灌注桩基础设计提供参考依据。     

城市客车七自由度平顺性模型仿真研究

建立某城市客车的七自由度平顺性模型,基于MATLAB/Simulink软件编写仿真程序和图形化界面,并进行仿真分析,将仿真结果与试验结果对比.     

Modern accumulation rates and a budget of sediment off the Gaoping (Kaoping) River, SW Taiwan: A tidal and flood dominated depositional environment around a submarine canyon

Ninety-two box cores collected during 2004–2006 from an area of ~ 3000 km² off the Gaoping (formerly spelled Kaoping) River, SW Taiwan, were analyzed for fallout radionuclides (²¹⁰Pb, ¹³⁷Cs and ⁷Be) to elucidate sedimentation rates and processes, and for the calculation of a sediment budget. The study area is located at an active collision margin with a narrow shelf and a submarine canyon extending essentially into the river's mouth. The results indicate fairly constant hemipelagic sedimentation in much of the open margin and for most of the time except in the inner shelf and along the axis of the canyon where sediment transport is more dynamic and is controlled by tidal current and wave activities constantly, and by fluvial floods or gravity-driven flows episodically. Sedimentation rates in the study area derived from ²¹⁰Pb and constrained by ¹³⁷Cs vary from 0.04 to 1.5 cm/yr, with the highest rates (> 1 cm/yr) flanking the Gaoping canyon over the upper slope (200–600 m) and the lowest rates (< 0.1 cm/yr) in the distal basin beyond the continental slope. The depocenter delineated from ²¹⁰Pb-based sedimentation rates overlaps with the area covered by a flood layer resulting from super-typhoon Haitang in July 2005. Such correspondence supports the notion that the processes operating on event timescale have bearing on the formation of the sediment strata over centennial or longer timescales.From the distribution of sedimentation rates, sediment deposited in the study area annually is estimated to be 6.6 Mton/yr, accounting for less than 20% of Gaoping River's sediment load. The calculated budget, coupled with the presence of the short-lived ⁷Be and non-steady-state distribution of low levels of ²¹⁰Pb in sediments along the canyon floor, suggests rapid transport of sediment from Gaoping River's mountainous watershed (the source) via the Gaoping (Kaoping) Submarine Canyon and adjacent channels (as the conduit and temporary sink) to the abyssal plain and the Manila Trench in the South China Sea (the ultimate sink).