键合纤维素衍生物手性固定相的合成及手性拆分

采用包夹聚合法,将纤维素(10-十一烯酸酯/3,5-二甲基苯基氨基甲酸酯)键合于乙烯基硅胶上,制备了键合纤维素(10-十一酸酯/3,5-二甲基苯基氨基甲酸酯)手性固定相(简称为键合纤维素(3,5-二甲基苯基氨基甲酸酯)(键合(CDMPC-CSP)),并对其进行了表征.分别以正己烷/异丙醇、正己烷/四氢呋喃、正己烷/三氯甲烷为流动相,对键合CDMPC-CSP的手性识别能力进行了评价.实验结果表明,键合CDMPC-CSP具有一定的手性识别能力,可以拆分所研究的8种手性化合物中的4种.     

考虑舰体变形时的捷联惯性系统初始对准方法

为尽可能消除惯性测量组件（IMU）安装误差及挠曲变形对初始对准精度的影响，运用传递对准技术，建立系统方程和量测方程，采用扩展状态滤波器和速度加角速率匹配的方法，准确地估计出了这些误差，并对系统进行补偿。仿真结果表明，用速度加角速率匹配估计安装误差和挠曲变形比用速度加姿态匹配效果好，补偿了安装误差和挠曲变形后，系统的导航精度明显提高。     

国际公路工程项目实施中的支付、赔偿与索赔

世行项目承包商在合同执行中,对支付与索赔尚缺乏全面了解与正确认识,经常误将一些支付、垫付偿还、赔偿补偿统统归为索赔,因而导致一些不必要的经济损失。简要介绍一些基本概念,侧重介绍在实践中如何应用这些知识解决支付、赔偿与索赔中的问题。     

高速电气化铁路的接触网电分相型式探讨

根据目前关节式电分相存在问题，提出一种新型的3个绝缘锚段关节双中性段关节式电分相型式，有效地克服了目前双锚段关节单中性段关节式电分相存在的问题，可较好解决关节式电分相对电力机车受电弓多弓运行条件的限制。     

Spatial distribution of cadmium over a cyclonic eddy in the southern East China Sea

Eddy systems are a unique ecosystem, usually having high biological masses and primary production in the sea. In this study, both particulate and dissolved phases of cadmium in the water column of 15 stations over a cyclonic eddy in the southern East China Sea were determined to obtain their spatial distributions. This allows us to confirm that cyclonic eddy systems play the role of a Cd pump in the sea.Results showed that particulate Cd (PCd) and dissolved Cd (DCd) concentrations in water varied greatly, ranging over two orders and one order of magnitude, respectively. Large spatial variability was found not only for PCd but also for DCd in the upper water, apparently due to the effects of the cyclonic eddy system on the Cd distributions over the study area. DCd accounts for about 99% of the total Cd. For the surface water, DCd concentration at the eddy center was about five times the average of the water surrounding the eddy center. The depth distributions of DCd exhibited a typical surface depletion and a subsequent increase with depth; however, the PCd distribution showed the opposite, i.e. a surface maximum and a subsequent decline with depth. In general, the DCd maxima were found at depths of 600–1000 m, agreeing well with the literature. It reflected the internal biogeochemical cycling of Cd in the water column, which was driven by the utilization of Cd by plankton in the euphotic zone and by the regeneration of Cd at depth. In addition, a remarkably high DCd concentration existed in near-bottom water around the cyclonic eddy center.The horizontal distributions of both PCd and DCd in the upper water shared a common feature with elevated concentrations centering around the eddy center and a decline in concentration with distance from the eddy center. This shows that the cyclonic eddy could bring up the Cd-rich deep water to the surface water around the eddy center and could then expand toward eddy's vicinity via advection–diffusion. It is thus likely that it produces ample biological masses over the eddy system. Hence, this work can demonstrate that the ascending nutrient-rich water driven by the cyclonic eddies can serve as an important source not only for many nutrients but also for Cd in the sea.     

用8098单片机实现电压空间矢量脉宽调制

电压空间矢量脉宽调制是一种先进的调制方法。本文介绍了其基本原理和输出电压，建立了开关模型和最佳开关顺序。分析了滞后开通时死区时间对输出电压的影响，提出了补偿方法，用８０９８单片机系统来实现电压空间矢量脉宽调制，具有简单，可靠的优点，试验结果证明，变频器运行稳定，输出波形正统性较好。     

CAN总线网络传输的延时优化研究

为减小CAN总线网络延时对传输速率的影响,提出了一种报文偏移量补偿与标识符优化的混合优化方案.首先定义总线网络传输延时,研究了表征CAN总线网络数据传输延时的主要指标,然后设计了报文分段与编码方案优化方法和延时报文的偏移量补偿方法,最后采用二者相结合的方案改善延时情况,并利用Symtavision软件分别对优化前、后C...