超声条件下超细铜粉的制备

在超声波条件下采用化学还原法,利用有机物为模板,制备了超细铜粉.通过X射线衍射仪和扫描电子显微镜,研究了超声条件及有机添加物的种类对产物的形貌和分散性能的影响.结果表明:超声波改善了铜粉产物的分散性,提高了铜粉颗粒的均匀度;表面活性剂组分变化极大地影响产物形貌,通过改变表面活性剂组分可将铜粉的形貌控制为类球状、片状或带状.     

裂解炉炉管吊耳弯头焊接裂纹产生原因分析

由于在更换文丘里管的施工中,吊耳弯头两端焊缝及母材不断产生裂纹,导致施工无法进行。通过研究吊耳弯头材质化学成分及焊缝的金相组织,找出产生焊接裂纹的原因。利用金相检验、化学成分分析、渗透检验等方法分别对母材及焊缝的开裂原因进行分析。结果表明：母材与焊缝附近开裂本质一致,都是源于热应力,在焊接状态下由于母材中碳和铜含量超标,造成母材脆性开裂。该批次吊耳弯头为不合格品,不能使用。     

Galvanic corrosion behaviour of aluminium 3004 and copper in tropical marine atmosphere

The galvanic corrosion behaviour of aluminium 3004 and copper with different area ratios were studied in the tropical marine atmosphere at Tuticorin harbour over a period of 426 days. The area ratios OfAAI： Acu, studied were l：l, 1：2, l：4, 1：8, 2：1, 4：1 ＆ 8：1. The galvanic corrosion behaviour of metals was studied in terms of relative increase in the corrosion rate of aluminium due to galvanic coupling with copper, relative decrease in the corrosion rate of copper due to galvanic coupling with aluminium, and the susceptibility of aluminium to pitting owing to galvanic coupling with copper, The galvanic potential and galvanic current of the system were monitored. Pits of different dimensions ranging from mild etchings to perforations were experienced on the borders and the surfaces of the interface of aluminium in contact with copper. The weathering parameters and the environmental pollutants which have a major role in influencing the galvanic corrosion of metals were also monitored. The corrosion products resulting from galvanic corrosion were analysed using XRD and the pitting on aluminium resulting from galvanic corrosion has been highlighted in terms of pit depth, size and density of pit, using a high resolution microscope.     

铜镍管直流脉冲TIG焊工艺试验与应用

为改善铜镍管焊接时的焊缝成形、提高焊接质量,选择手工直流脉冲钨极惰性气体(Tungsten Inert Gas,TIG)焊并采取无间隙组对进行工艺试验。经相关检测,焊后内外焊缝成形优良,表面无缺陷,X射线探伤满足规范要求。试验结果表明:采用手工直流脉冲TIG焊可有效改善管子内壁焊缝成形、减少焊接缺陷、提升焊接质量;采取无装配间隙的组对方式可提高管子零件的制作精度与工作效率,在实船应用中得到推广并取得较好的效果。