键合纤维素衍生物手性固定相的合成及手性拆分

采用包夹聚合法,将纤维素(10-十一烯酸酯/3,5-二甲基苯基氨基甲酸酯)键合于乙烯基硅胶上,制备了键合纤维素(10-十一酸酯/3,5-二甲基苯基氨基甲酸酯)手性固定相(简称为键合纤维素(3,5-二甲基苯基氨基甲酸酯)(键合(CDMPC-CSP)),并对其进行了表征.分别以正己烷/异丙醇、正己烷/四氢呋喃、正己烷/三氯甲烷为流动相,对键合CDMPC-CSP的手性识别能力进行了评价.实验结果表明,键合CDMPC-CSP具有一定的手性识别能力,可以拆分所研究的8种手性化合物中的4种.     

基于MATLAB复调制ZOOM-FFT算法的分析和实现

频谱细化技术近年来发展迅速，常见方法有：基于复调制的Zoom-FFT法、Chirp-Z变换、Yip-Zoom变换等。从分析精度、计算效率、分辨率、灵活性等方面来看，基于复调制的Zoom-FFT方法是一项行之有效的方法，因而也得到了比较广泛的应用。在介绍复调制Zoom-FFT算法基本原理的基础上，用Matlab实现该算法，并通过仿真进行验证，表明该算法简明、易实现。最后讨论算法的运算量和局限性。     

船舶发电机组并联时运行负载自动转移故障分析

通过对某船舶发电机并联运行负载自动转移原因的分析,总结了船舶发电机组液压调速器日常管理和维护保养的一些经验。     

高速电气化铁路的接触网电分相型式探讨

根据目前关节式电分相存在问题，提出一种新型的3个绝缘锚段关节双中性段关节式电分相型式，有效地克服了目前双锚段关节单中性段关节式电分相存在的问题，可较好解决关节式电分相对电力机车受电弓多弓运行条件的限制。     

Spatial distribution of cadmium over a cyclonic eddy in the southern East China Sea

Eddy systems are a unique ecosystem, usually having high biological masses and primary production in the sea. In this study, both particulate and dissolved phases of cadmium in the water column of 15 stations over a cyclonic eddy in the southern East China Sea were determined to obtain their spatial distributions. This allows us to confirm that cyclonic eddy systems play the role of a Cd pump in the sea.Results showed that particulate Cd (PCd) and dissolved Cd (DCd) concentrations in water varied greatly, ranging over two orders and one order of magnitude, respectively. Large spatial variability was found not only for PCd but also for DCd in the upper water, apparently due to the effects of the cyclonic eddy system on the Cd distributions over the study area. DCd accounts for about 99% of the total Cd. For the surface water, DCd concentration at the eddy center was about five times the average of the water surrounding the eddy center. The depth distributions of DCd exhibited a typical surface depletion and a subsequent increase with depth; however, the PCd distribution showed the opposite, i.e. a surface maximum and a subsequent decline with depth. In general, the DCd maxima were found at depths of 600–1000 m, agreeing well with the literature. It reflected the internal biogeochemical cycling of Cd in the water column, which was driven by the utilization of Cd by plankton in the euphotic zone and by the regeneration of Cd at depth. In addition, a remarkably high DCd concentration existed in near-bottom water around the cyclonic eddy center.The horizontal distributions of both PCd and DCd in the upper water shared a common feature with elevated concentrations centering around the eddy center and a decline in concentration with distance from the eddy center. This shows that the cyclonic eddy could bring up the Cd-rich deep water to the surface water around the eddy center and could then expand toward eddy's vicinity via advection–diffusion. It is thus likely that it produces ample biological masses over the eddy system. Hence, this work can demonstrate that the ascending nutrient-rich water driven by the cyclonic eddies can serve as an important source not only for many nutrients but also for Cd in the sea.     

我国兆瓦级交流牵引传动系统的试验研究

本文叙述了我国迄今功率最大的交流传动系统的地面试验结果。作为研制大功率交流传动干线电力机车的基础研究,所进行的试验研究对象包括四象限脉冲整流器、中间直流电路和脉宽调制逆变器,即为交-直-交电压型变流器,同时还研制了适合机车牵引用的电子控制装置。文中阐述了交流传动电力机车的特征、试验系统的方案选择、系统及部件的设计原理,最后给出了系统试验结果,包括1025kW的牵引特性、800kW的再生制动特性以及有关数据。     

用8098单片机实现电压空间矢量脉宽调制

电压空间矢量脉宽调制是一种先进的调制方法。本文介绍了其基本原理和输出电压，建立了开关模型和最佳开关顺序。分析了滞后开通时死区时间对输出电压的影响，提出了补偿方法，用８０９８单片机系统来实现电压空间矢量脉宽调制，具有简单，可靠的优点，试验结果证明，变频器运行稳定，输出波形正统性较好。     

湿式双离合器自动变速器换挡规律制定与验证

建立基于油门开度和车速的最佳动力性和最佳经济性换挡规律,根据车辆不同挡位和油门开度,车辆对动力性和经济性要求的不同,对所建立的最佳动力性和经济性换挡规律进行调整,得到综合换挡规律。建立整车仿真模型,完成基于dSPACE的综合换挡规律快速原型试验,验证了综合换挡规律的正确性。