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双层Ni-P合金镀层制备及耐蚀性 总被引:1,自引:0,他引:1
为研究双层Ni-P合金镀层的高耐蚀性,通过改变络合剂组分和控制化学镀工艺条件,制备了3种不同磷含量的镀层.用XRD,EDS和SEM方法,对镀层的成分、结构和形貌进行表征,并用电化学方法和腐蚀膏法,分别测定了镀层的腐蚀电位和耐蚀性.结果表明:不同的镀液成分和化学镀工艺使镀层的磷含量和组织结构发生变化.随镀层中磷含量上升,镀层组织的变化从晶态到晶态+非晶态,最后到非晶态,使镀层的自腐蚀电位及自腐蚀电流分别增加和下降.在外层为低电位层(-550 mV),内层为高电位层(-295 mV),内外层厚度比为2∶1时,镀层的耐腐蚀性最好. 相似文献
177.
采用电化学方法测定一种Fe-Mn-Al-Cr合金在模拟PEMFC环境中的极化曲线以及在PEMFC工作电位下的电流密度随时间变化的曲线.结果表明,Fe-Mn-Al-Cr合金在0.05 mol/L H2SO4+2 mg/L F-溶液中呈现明显的活化-钝化转变.在恒电位极化过程中,阴极一侧表面能够形成稳定的钝化膜,钝化电流密度低于l6μA.cm-2.而在阳极一侧则产生了大量溶解的金属离子. 相似文献
178.
Recycling of aluminum alloy scrap obtained from delaminated fibre metal laminates (FMLs) was studied through high temperature refining in the presence of a salt flux. The aluminum alloy scrap contains approximately mass fraction w(Cu) = 4.4%, w(Mg) = 1.1% and w(Mn) = 0.6% (2024 aluminum alloy). The main objective of this research is to obtain a high metal yield, while maintaining its original alloy compositions. The work focuses on the metal yield and quality of recycled Al alloy under different refining conditions. The NaCl-KCl salt system was selected as the major components of flux in the Al alloy recycling. Two different flux compositions were employed at NaCl to KCl mass ratios of 44:56 and 70:30 respectively, based on either the eutectic composition, or the European preference. Different additives were introduced into the NaCl-KCl system to study the effect of flux component on recycling result. Although burning and oxidation loss of the alloying elements during re-melting and refining take place as the drawbacks of conventional refining process, the problems can be solved to a large extent by using an appropriate salt flux. Experimental results indicate that Mg in the alloy gets lost when adding cryolite in the NaCl-KCl salt system, though the metal yield can reach as high as 98%. However, by adding w(MgF2) = 5% into the NaCl-KCl salt system (instead of using cryolite) all alloying elements were well controlled to its original composition with a metal yield of almost 98%. 相似文献
179.
Formation of nanometer coherent structures during spinodal decomposition and ordering coexistence phase transformation in Fe-24Al alloys 总被引:1,自引:0,他引:1
The nanometer coherent structure evolution of spinodal decomposition and ordering coexistence phase transformation in Fe-24Al alloys is investigated by the microscopic phase field kinetic model. The results show that the concentration and long-range order parameters all continuously change towards to their equilibrium values during phase transformation. With the increase of elastic interaction energy, the anisotropy along [01] or [10] elastic soft direction is more obvious and the time reaching equilibrium state is also shortened. According to the results, the formation of nanometer coherent structures during phase transformation is composed of the initial decreasing stage of order degree stage, the incubation stage, the continuous increasing stage of concentration order parameter and long-range order parameter, and the later stable stage. The spinodal decomposition and ordering is interaction; the initial ordering stage is a necessary condition of the coexistence phase transformation. The nanometer coherent structures are not found to grow during the whole phase transformation. The simulation results are in accordance with the results in experiment obtained by the aging treatment in Fe-24Al alloys. 相似文献
180.
在氩气保护下,应用真空熔炼炉分别制备了Ni30Mn70与Ni55Mn45合金.测定了这两种合金在(NH4)2SO4溶液中的圾化曲线,然后对其进行去合金化实验.结果显示,Ni30Mn70合金在1M(NH4)2S04溶液中去合金化后,试样表面呈现“泥裂”结构.Ni55Mn45在1M(NH4)2S04溶液中不同电位下去合金化... 相似文献