用光学混合方法测定GaAs的输运参量

本文提出了用光学混合技术测定光电导材料输运参量的新方法，He-Ne激光的多纵模在n型GaAs样品上的混合，可获得该样品的光电流和三倍差频的微波功率信号，经把光电导外差分析方法推广后，可得出载流子寿命、迁移率、漂移速度等参量对所加电场的依赖关系和它们的温度特性，并在20K-240K的温度区间，讨论了该样品的复合机构和散射机构。     

用吸光度法对正常He青年人咀嚼效能的测定与分析

研究影响咀嚼效能的因素。方法采用吸光度法来测定１８名正常Ｈｅ青年人在自由咀嚼状态下的半分钟咀嚼效能、吞咽反射前咀嚼效能以及限定用单侧咀嚼的半钟喟嚼效能。     

天津新港抛泥区泥沙运动规律分析

天津新港抛泥地的泥沙运动以往研究较少，其泥沙运动对航道的影响不说，本文利用现场实测资料，对抛泥区的潮流特征、泥沙运动规律作以分析研究，并首次在国内试用中子活化技术对底沙运动进行了示踪测定。     

高锰酸盐指数影响因素研究

影响高锰酸盐指数测定结果的因素较多,导致测定结果的准确度较差。为提高高锰酸盐指数测定结果的准确性,本文对影响测定结果的三个主要因素包括取样量、加热时间和高锰酸钾标准滴定溶液的浓度进行了实验和研究。结果表明,实验过程中必须严格控制以上各实验条件,如取样量为100mL,加热时间尽量准确控制在30min,高锰酸钾标准滴定溶液的浓度控制在0.0098mol/L～0.0100mol/L之间等。     

Analysis and determination of diterpenoids in unprocessed and processed Euphorbia lathyris seeds by HPLC-ESI-MS

Euphorbia lathyris （Caper spurge） is a toxic and potent Chinese materia medica （T/PCMM）. This study sought a method for identifying five diterpenoids （Euphorbia factors LI-L3, L7a, and Ls） with the spectra of UV and mass, quantifying three diterpenoids L1, L2, and L8 in crude extracts of unprocessed and processed E. lathyris seeds by liquid chromatography/ electrospray ionization mass spectrometry （LC-ESI-MS）. The analysis was achieved on an Agilent Eclipse XDB-C18 column （4.6 mm× 150mm i.d., 5 μm） with an isocratic elution with a mobile phase consisting of water and acetonitrile at a flow rate of 0.25 mL/min at column temperature of 30 ℃ and UV detection was set at 272 nm. An ESI source was used with a positive ionization mode. The calibration curve was linear in the ranges of 9.9-79 μg/mL for Euphorbia factor Lb 3.8-30.5μg/mL for Euphorbia factor L2, and 1.0-20.6 μg/mL for Euphorbia factor LB. The average recoveries （n=6） of three diterpenoids were 98.39%, 91.10% and 96.94%, respectively, with RSD of 2.5%, 2.4% and 2.1%, respectively. The contents of the three diterpenoids in processed E. lathyris seeds were 3.435, 1.367 and 0.286 mg/g, respectively, which decreased more sharply than those in unprocessed E. lathyris seeds which were 4.915, 1.944 and 0.425 mg/g, respectively. The method is simple, accurate, reliable and reproducible, and it can be applied to control the quality of unprocessed and processed E. lathyris seeds.     

Rapid europium-sensitized fluorescent determination of ulifloxacin,the active metabolite of prulifloxacin,in human serum

A new fluorescent method was developed based on the ulifloxacin-europium（Ⅲ）-sodium dodecylbenzene sulfonate system for the determination of ulifloxacin,the active metabolite of prulifloxacin.Sodium dodecylbenzene sulfonate formed a ternary complex with ul     

Determination of phthalate esters in physiological saline solution by monolithic silica spin column extraction method

Monolithic silica spin column extraction （MonoSpin-SPE） was developed as a simple, sensitive, and eco-friendly pretreatment method which combined with ultra-fast liquid chromatography-mass spectrometry （UFLC-MS） to determine the levels of six phthalate es     

博世氧传感器必有一款合适您

为精确测定尾气排放，各整车厂为每一台发动机都装备了一款适用的氧传感器，这意味着在售后市场需要许多型号的氧传感器。当维修站更换氧传感器时，需要更换与原厂氧传感器功能完全相同的氧传感器。做到这一点，对于任何一个汽车零配件供应商来说都是巨大的挑战。博世氧传感器产品系列完全可以满足售后市场的这一富有挑战性的要求：     

Determination of metronidazole in a rat stomach by HPLC for obtaining basic data of the eradication therapy of Helicobacter pylori

In the eradication therapy of Helicobacter pylori changes of antibiotics as these concentrations or amount in the stomach after oral administration were not clear. A simple and accurate method for dete...