软体排深水沉放结构受力试验分析

通过室内模型试验，测定软体排在静水，动水中的结构受力，结合软体排实际辅设过程中冲刷变形态势。分析软体排在沉放过程中的受力状况。     

五问五答

1.为什么车的不同部位要用不同的油？答：因为汽车的不同部位结构和工作原理不同,其润滑方式也不同,所以不同部位要用不同种类的润滑油。例如,发动机中用内燃机油;手动变速器和差速器中用齿轮油。     

卵巢癌标志抗原CA125检测的临床价值

用 McAb固相放射免疫技术对26例妇科肿瘤、包块（含13例卵巢癌）及5例正常对照进行CA125检测,并与CEA、AFP对照。结果:①卵巢上皮癌12例均显著升高,CEA仅2/12增高;②手术或化疗后短期内CA125并不都迅即降低,有的反见升高;③作为术后监测,CA125可先于临床复发前半年即升高;④CA125和CA19-9等抗原在某些病例可同时升高,提示肿瘤标记的复杂多样性。     

太白蓼的生药学研究

作者对陕西特有民间药太白蓼(Polygonum taipaishanense Kung.)从来源、药材性状、显微组织结构、粉末特征和理化鉴定等方面进行了系统的生药学研究,同时进行了鞣质定性及含量测定,为太白蓼的鉴别、品质评价、质量标准的制定及进一步的开发利用提供了科学依据。     

石煤发热量的快速直接测定

快速直接测定法是通过调整内外筒温差，使△ｔ近似等于零，将非绝热式热量计当成绝热式热量计应用，不锈钢坩埚底部打孔，使氧气上下对流，煤层供氧充分而能完全燃烧，此法实现了低热值石煤也能直接点火燃烧测定，同时取消了本特法测定过程中的初期和末期，免去了△ｔ的计算，简化了分析手续，大大缩短了分析时间。     

Synthesis of a new chitosan derivative and assay of Escherichia coli adsorption

A new chitosan derivative is prepared using chitosan.Ethyl chlorocarbonate was first introduced to the hydroxyl group of phthaloylchitosan through a nucleophilic reaction.Hydrazine was then added to recover the amino groups of chitosan and promote cross-l     

Rapid europium-sensitized fluorescent determination of ulifloxacin,the active metabolite of prulifloxacin,in human serum

A new fluorescent method was developed based on the ulifloxacin-europium（Ⅲ）-sodium dodecylbenzene sulfonate system for the determination of ulifloxacin,the active metabolite of prulifloxacin.Sodium dodecylbenzene sulfonate formed a ternary complex with ul     

Determination of phthalate esters in physiological saline solution by monolithic silica spin column extraction method

Monolithic silica spin column extraction （MonoSpin-SPE） was developed as a simple, sensitive, and eco-friendly pretreatment method which combined with ultra-fast liquid chromatography-mass spectrometry （UFLC-MS） to determine the levels of six phthalate es     

Analysis and determination of diterpenoids in unprocessed and processed Euphorbia lathyris seeds by HPLC-ESI-MS

Euphorbia lathyris （Caper spurge） is a toxic and potent Chinese materia medica （T/PCMM）. This study sought a method for identifying five diterpenoids （Euphorbia factors LI-L3, L7a, and Ls） with the spectra of UV and mass, quantifying three diterpenoids L1, L2, and L8 in crude extracts of unprocessed and processed E. lathyris seeds by liquid chromatography/ electrospray ionization mass spectrometry （LC-ESI-MS）. The analysis was achieved on an Agilent Eclipse XDB-C18 column （4.6 mm× 150mm i.d., 5 μm） with an isocratic elution with a mobile phase consisting of water and acetonitrile at a flow rate of 0.25 mL/min at column temperature of 30 ℃ and UV detection was set at 272 nm. An ESI source was used with a positive ionization mode. The calibration curve was linear in the ranges of 9.9-79 μg/mL for Euphorbia factor Lb 3.8-30.5μg/mL for Euphorbia factor L2, and 1.0-20.6 μg/mL for Euphorbia factor LB. The average recoveries （n=6） of three diterpenoids were 98.39%, 91.10% and 96.94%, respectively, with RSD of 2.5%, 2.4% and 2.1%, respectively. The contents of the three diterpenoids in processed E. lathyris seeds were 3.435, 1.367 and 0.286 mg/g, respectively, which decreased more sharply than those in unprocessed E. lathyris seeds which were 4.915, 1.944 and 0.425 mg/g, respectively. The method is simple, accurate, reliable and reproducible, and it can be applied to control the quality of unprocessed and processed E. lathyris seeds.