磷酸铵镁技术中不同沉淀剂脱氮除磷效果比较

探讨了磷酸铵镁法中不同沉淀剂的脱氮除磷效果,比较了氨氮去除率、磷酸盐去除率、残氮量、残磷量,沉淀物质质量和组成,处理液的电导率。综合考虑了各方面因素得出处理高浓度氨氮废水的较佳的沉淀剂为Na3PO.412H2O MgCl2.6H2O和Na3PO4.12H2O MgSO4.7H2O,处理高浓度磷酸盐废水的较佳的沉淀剂为NH4Cl MgCl2.6H2O和NH4Cl MgSO.47H2O.并对磷酸铵镁沉淀进行了X-衍射光谱和扫描电镜表征。     

THE STUDY ON THE CHANGES OF ZINC, COPPER, CALCIUM AND MAGNESIUM IN PLASMA AND ERYTHROCYTES DURING CARDIOPULMONARY BYPASS

Objective To study the changes and their influence factors involved of zinc, copper, calcium and magnesium in plasma and erythrocytes during cardiopulmonary hypass(CPB). Methods Zinc, copper, calcium and magnesium values in plasma and erythrocytes were measured by atomic absorption spectrophotometer during CPB. Results Zinc and copper levels in plasma were significantly elevated above preinduction level before perfusion, hut calcium and magnesium levels did not change significantly; zinc, copper and calcium levels in plasma were significantly below preoperation level during CPB, hut magnesium level in plasma was significantly increased above preoperation; zinc level in plasma was increased to preoperation level after CPB and began to decrease again at 8 hours after CPB,copper level in plasma was increased to preoperation level at 20 hours after CPB, calcium in plasma was increased significantly from beginning to 8 hours after CPB, magnesium level in plasma was decreased to preoperation level at 8 hours afterCPB. Concentration of zinc , copper, calcium and magnesium in erythrocytes did not change significantly. Conclusion During CPB, the changes of zinc, copper, calcium and magnesium had relation to hemodilution, operative wound, carrier protein, stress and component of priming Solution and cardioplegic solution, hut no relation to transferfrom plasma erythrocytes. The results indicate that it is beneficial to patient‘s recovery to supplement zinc, copper, calcium and magnesium properly by different ways during cardiac perioperation.     

有效钙镁含量及灰土中灰剂量测定的技术关键

结合试验规程及实践经验,阐述了石灰有效钙镁含量及灰土中灰剂量测定的原理,指出了关键点、注意点,介绍了公式的由来,有利于提高试验的准确度.     

海绵钛的表面活性与氢化动力学

本文研究了真空热处理对海绵钛氢化动力学的影响。为了清洁和活化样品表面，把样品置于473K，10^-1Pa的低真空状态下，以不同的时间周期对其进行退火处理。经过这一步之后，样品在623K、773K和1073K温度下被氢化。我们发现在773K和1073K时，样品的预处理对Ti的氢化动力学并没有影响，这一过程受到氢在钛中体扩散的控制。另一方面，在623K时，样品的氢化存在一个孕育时间(腔内氢压力不变)，接着对应于表面控制过程，压力直线下降，对应氢的体扩散压力呈抛物线状。在623K时吸氢的孕育时间与在473K时的活化时间有关。这种相互关系被解释成认为与清洁阶段的两个机械操作过程有关，一是吸入的气体从Ti的空洞中被释放从而留下了清洁的钛表面，另一种是清洁的表面被氧化。     

磷酸铵镁技术影响因素的优化

通过正交实验得出影响氨氮和磷酸盐去除率因素的主次顺序为:浓度＞pH＞ Mg∶N ＞P∶N＞反应时间.通过一次回归正交实验得出残磷量和残氮量的回归方程为:y(残磷量)=-3041.57-2.76z1 +2307.2z2 +3075.5z3-2 310z2z3(其中z1=pH,z2=Mg∶N,z3=P∶N),y(残氮量)=1 104.84 - 50.76z1- 45.5z2 - 515.5z3,回归方程高度显著.在氨氮浓度为0.1 mol/L(1 400 mg/L)及磷酸盐为相应浓度时,在兼顾处理出水的含盐量、残磷量和残氮量尽量低的前提下,最佳的实验条件为:pH=9.5,Mg∶N=1.2,P∶N=     

Ignition-proof properties of a high-strength Mg-Gd-Ag-Zr alloy

<正>A high-strength Mg-15.3Gd-l.8Ag-0.3Zr(GQ152K,mass fraction) alloy was prepared by conventional ingot metallurgy process.The solution and aging(denoted as T6) treated alloy exhibits remarkable mechanical properties with ultimate tensile strength of 421 MPa and tensile yield strength of 309MPa.It has higher igniting temperature of 1208 K.Moreover,it can stand against flame at 1203 K for over 6 min in vertical burning tests, and its flammabiUty behavior is very similar to that of 6101A1 alloy.Vertical burning tests appear to be able to directly study the flammability behavior of Mg alloys and it appears to be a good approach to study the flammability behavior of Mg alloys in an aircraft fire accident.     

陕西省长寿区老人血清中锰、铜、锌、铁及钙、镁的分析

作者对陕西省长寿区老人血清中微量元素(锰、铜、锌、铁)及钙、镁进行分析。发现陕西省长寿区老人血清中利于健康长寿的锰的含量极显著地高于对照区(P<0.001);人体必需的铜的含量也极显著地高于对照区(P<0.01);与抗衰老关系密切的钙的含量也极显著地高于对照区(P<0.01);男性老人血清中锰、铜、锌、铁及钙、镁的含量与女性老人均无显著差异;61岁～90岁的老人血清中锰、铜、锌、铁及钙、镁的含量随着年龄的增长也均未有显著差异。结果表明陕西省长寿区老人血清中有较优越的化学元素谱。本文对实验结果中与抗衰老有关问题进行了讨论。     

膨胀剂与纤维增强混凝土抗裂性的研究

通过掺加钙镁膨胀剂和玄武岩纤维,采用单轴拉伸试验研究了混凝土的应力应变,探究了不同组分、掺量和水胶比对混凝土抗裂性的影响,确定了掺膨胀剂和纤维抗裂混凝土轴向拉伸应力-应变曲线数学表达式。研究表明：添加膨胀剂和玄武岩纤维可提高混凝土的抗拉强度和韧性,纤维和膨胀剂掺量为1%和7%,水胶比为0.42,混凝土抗裂性能较好,得到的本构方程与试验结果基本吻合,可为抗裂混凝土的研究和应用提供了理论依据。     

粒化高炉矿渣改性磷酸镁水泥抗冻性能试验研究

磷酸镁水泥（MPC）作为一种早强、快硬新型胶凝材料而受到广泛关注,但其抗冻性较差,致使在严寒条件下使用受到限制。以粒化高炉矿渣（GGBS）作为改性剂取代一定数量的重烧氧化镁（MgO）制备水泥,得到MPC-GGBS复合水泥。通过水泥砂浆冻融循环试验,测试MPC-GGBS水泥砂浆冻融循环后的质量损失率、强度和强度保留率;并通过SEM-EDS测试,分析GGBS对MPC抗冻性能影响。结果表明：当GGBS掺量在36%时,MPC-GGBS复合水泥砂浆冻融循环后具有最小的质量损失率和最高的强度保留率,且MPC-GGBS水泥砂浆与波特兰水泥砂浆基体之间的粘结强度最大;SEM-EDS分析表明,GGBS的掺入可填充砂浆孔隙,提高了砂浆的致密性和整体性,且生成大量的AFt和AH₃胶凝材料,从而使MPC抗冻性能显著提升。