8-羟基喹啉铝晶体的制备与表征

报道了制备较高纯度有机电致发光材料8-羟基喹啉铝(Alq3)及其微晶的方法;通过X射线衍射谱(XRD)、红外吸收光谱、荧光光谱及扫描电子显微镜(SEM)测试分析,对Alq3微晶的结构和特性进行了表征。XRD证实了微晶主要成份为α-Alq3,并含有少量δ-Alq3;红外吸收光谱显示,Al-N键的伸缩振动模式对应谱峰407 cm-1,418 cm-1处,Al-O键的伸缩振动模式对应谱峰523 cm-1,542 cm-1,548 cm-1处,说明晶体中N、O分别与Al3+发生了配位,标定了微晶中喹啉环的存在;荧光光谱检测得到Alq3微晶在固态、(氯仿)溶液中的荧光发射谱峰分别位于500 nm、512 nm处;通过SEM观测了Alq3微晶的形貌,分析得到Alq3晶粒呈现六方形结构。     

基于Visual C＋＋与K-803B8焊接温度测量仪的设计

阐述了自动温度测量仪的基本硬件结构组成和工作原理,测温系统硬件组成简单,测温仪软件程序利用Visual C++编写,界面友好,适合各阶层人用,经测试该测量仪具有良好的测量精度和实时传输功能,性能稳定,具有方便携带,即插即用等特点.     

Experimental study on responses of an 8-module VLFS considering different encounter wave conditions

For the very large floating structure (VLFS) which is deployed near seashores, islands and reefs, the encounter wave conditions are always extremely complex. Traditional methods using homogeneous wave environment conditions cannot be applied for the analysis. In order to provide references for the further development of numerical methods, this paper reports an experimental study on responses of an 8-module VLFS under three different encounter wave conditions. The wave heights, accelerations, motions and connector loads of VLFS in three test schemes are obtained and analyzed. The comparative results show that the inhomogeneous wave conditions have an essential influence on the responses of VLFS. Especially for the connector loads, the values in the inhomogeneous wave conditions increase a lot compared with the other two test schemes. It indicates the traditional numerical methods using homogeneous wave field may not guarantee a safe design of VLFS and its connectors in the complicated wave environments.     

DF8CJ型机车斜齿轮变速箱的设计

对直齿轮变速箱存在的各种问题进行了分析,提出了采用斜齿轮变速箱的解决方案。将直齿轮传动改为斜齿轮传动,消除异音、降低噪音;增加齿轮油泵,加强了润滑;采用全新油封结构,增强密封性能。     

8K机车904^#开关电源板的国产化研制

介绍了采用零电流开关变流技术研制8K机车904^#开关电源板,设计采用了模块化结构,从而提高了电源板使用的可靠性。通过微处理器软件编程技术实施对输入、多输出电源进行管理,不仅提高了对电源故障监控的准确性和响应速度,而且提高了对电源故障维修处理的效率。     

SS8型电力机车横向稳定性计算分析

着重对ＳＳ８型电力机车的横向稳定性进行了计算，分析了机车各主要参数对失稳临界速度的影响。计算分析结果表明，当踏面斜度为０．４时，机车失稳的临界速度大于１９０ＫＭ／ｈ。     

两种提速型转向架侧架的强度分析

针对目前提速使用的设计时速为100 km/h的转8AG型和转8G型货车转向架侧架,采用有限元分析方法进行静强度计算.分析结果表明,转8AG型和转8G型货车转向架侧架整体上满足强度要求,应力最大部位发生在承台拐角、轴箱拐角和三角透视孔部位,这些部位在车辆实际运行中应给予重点关注.对转8AG型侧架进行了静强度测试,测试结果与计算结果基本一致.同时对转8AG型和转8G型侧架进行了比较分析,结果表明,转8G型侧架的强度指标明显优于转8AG型侧架.     

Measurement of Swarm Parameters of c-C4F8/CO2 and Its Insulation Characteristics Analysis

In c-C4F8 and c-C4F8/CO2 mixtures, the swarm parameters including ionization coefficient, attachment coefficient and effective ionization coefficient were obtained at the ratio of the electric field strength to the gas density between 150-550 Td by the steady-state Townsend (SST) method. Static breakdown voltages at each ratio were also measured at the SST condition. The limiting field strengths were obtained by two methods:computing the density-normalized effective ionization coefficient as a function of the overall density-reduced electric field strength; and measuring static breakdown voltages as a function of the product of gas density and electrode separation. Good agreement was obtained by these two methods, which ensures the correctness of the former method. The limiting field strengths of c-C4F8 and c-C4F8/CO2 mixtures were compared with those ofpure SF6, SF6/CO2 mixtures and pure c-C4Fs. It is found that buffer gas CO2 does not reduce the limiting field strengths of c-C4F8 greatly, the limiting field strengths of c-C4F8/CO2 mixtures are higher than those of SF6/CO2 mixtures or even pure SF6, and so c-C4F8/CO2 mixtures are suggested to be possible substitutes for SF6.     

Insulin-3基因敲除鼠生殖系统LGR8蛋白的表达

目的 Insulin-3(Insl3)和其唯一配体富含亮氨酸的G蛋白受体[LGR8(aka RXFP2)]系统在睾丸下降过程中起重要作用。本研究拟利用Insl3基因敲除鼠探讨Insl3与LGR8相互关系及其在生殖系统的表达情况。方法使用免疫共沉淀、Western blot及免疫组化法检测雄性野生型小鼠和Insl3基因敲除雄性小鼠各生殖器官LGR8蛋白的表达并比较分析。结果 LGR8蛋白在野生型小鼠睾丸、睾丸引带、附睾及输精管等多个雄性生殖器官均有表达。其表达程度在不同生殖器官不同,野生型小鼠睾丸LGR8的表达强于Insl3基因敲除鼠(P<0.05)。结论 LGR8蛋白在多个雄性生殖器官均有表达,Insl3-LGR8系统可能在男性多种生殖发育疾病中起作用。     

网压突降引起8K机车再生过流分析及恢复换相电路介绍

本文对8K机车在再生制动工况下,因网压突降导致再生失败的原因进行了分析,并对其改进电路——恢复换相电路的工作原理作了详细介绍。这一改进对目前国产再生机车的设计具有一定的参考价值。