吸能转向柱临界压缩力的设定

为防止或减少汽车碰撞对驾驶员的伤害,吸能转向柱得到广泛应用。文章通过对安全气囊气体发生器的反作用力和碰撞时方向盘下缘所受撞击力的分析,结合碰撞中不同情况下乘员头部和胸部对转向柱的撞击情况,确定了不同工况对吸能转向柱临界压缩力设定的影响,并最终指出如何结合安全带的选用及安全气囊的匹配情况来设定吸能转向柱的临界压缩力。     

Analysis and determination of diterpenoids in unprocessed and processed Euphorbia lathyris seeds by HPLC-ESI-MS

Euphorbia lathyris （Caper spurge） is a toxic and potent Chinese materia medica （T/PCMM）. This study sought a method for identifying five diterpenoids （Euphorbia factors LI-L3, L7a, and Ls） with the spectra of UV and mass, quantifying three diterpenoids L1, L2, and L8 in crude extracts of unprocessed and processed E. lathyris seeds by liquid chromatography/ electrospray ionization mass spectrometry （LC-ESI-MS）. The analysis was achieved on an Agilent Eclipse XDB-C18 column （4.6 mm× 150mm i.d., 5 μm） with an isocratic elution with a mobile phase consisting of water and acetonitrile at a flow rate of 0.25 mL/min at column temperature of 30 ℃ and UV detection was set at 272 nm. An ESI source was used with a positive ionization mode. The calibration curve was linear in the ranges of 9.9-79 μg/mL for Euphorbia factor Lb 3.8-30.5μg/mL for Euphorbia factor L2, and 1.0-20.6 μg/mL for Euphorbia factor LB. The average recoveries （n=6） of three diterpenoids were 98.39%, 91.10% and 96.94%, respectively, with RSD of 2.5%, 2.4% and 2.1%, respectively. The contents of the three diterpenoids in processed E. lathyris seeds were 3.435, 1.367 and 0.286 mg/g, respectively, which decreased more sharply than those in unprocessed E. lathyris seeds which were 4.915, 1.944 and 0.425 mg/g, respectively. The method is simple, accurate, reliable and reproducible, and it can be applied to control the quality of unprocessed and processed E. lathyris seeds.     

Development of the fingerprints for the quality evaluation of Viscum coloratum by high performance liquid chromatograp

A high-performance liquid chromatography coupled ultraviolet （HPLC-UV） method was developed for a chemical fingerprint analysis of Viscum coloratura. Eighteen peaks were selected as the common peaks and Homoeriodictyol-7-O-β-D-apiosiyl-（1→2）-β-D-glucoside     

瓦窑岭瓦斯隧道施工通风技术

通过瓦窑岭瓦斯隧道施工通风设计,介绍了高瓦斯隧道施工期间方案、通风计算、风机的选型、瓦斯的处置措施以及施工经验总结。     

双燃料发动机电力推进LNG船可燃气体探测系统设计简介

详细介绍了双燃料发动机电力推进LNG船可燃气体探测系统设计的基本要求,包括可燃气体探头及取样管在不同区域的布置情况及数量要求。所述内容不仅涉及LNG船本身的要求,也覆盖了其他类型的液化气体运输船的相关要求。     

转炉煤气中O_2气体分析系统设计

通过分析煤气回收工艺,介绍了炼钢厂转炉煤气中O2气体分析系统,包括取样单元、样品传输单元、样品预处理单元、分析单元。O2气体分析系统安装在气化装置的现场,设置了现场分析防护室,为其提供良好的运行环境和特殊的防护,以确保实时、准确地检测出转炉煤气中O2的含量。     

Gas transfer velocities of CO2 and CH4 in a tropical reservoir and its river downstream

We have measured simultaneously the methane (CH₄) and carbon dioxide (CO₂) surface concentrations and water–air fluxes by floating chambers (FC) in the Petit-Saut Reservoir (French Guiana) and its tidal river (Sinnamary River) downstream of the dam, during the two field experiments in wet (May 2003) and dry season (December 2003). The eddy covariance (EC) technique was also used for CO₂ fluxes on the lake. The comparison of fluxes obtained by FC and EC showed little discrepancies mainly due to differences in measurements durations which resulted in different average wind speeds. When comparing the gas transfer velocity (k₆₀₀) for a given wind speed, both methods gave similar results. On the lake and excluding rainy events, we obtained an exponential relationship between k₆₀₀ and U₁₀, with a significant intercept at 1.7 cm h^− 1, probably due to thermal effects. Gas transfer velocity was also positively related to rainfall rates reaching 26.5 cm h⁻¹ for a rainfall rate of 36 mm h^− 1. During a 24-h experiment in dry season, rainfall accounted for as much as 25% of the k₆₀₀. In the river downstream of the dam, k₆₀₀ values were 3 to 4 times higher than on the lake, and followed a linear relationship with U₁₀.     

Comparison of HC species from diesel combustion modes and characterization of a heat-up doc formulation

This study summarizes engine speed and load effects on HC species emissions from premixed charge compression ignition (PCI) and conventional diesel combustion, and it evaluates diesel oxidation catalyst (DOC) formulations on a gas flow reactor for the purpose of diesel particulate filter regeneration or lean NO_x trap desulfation. HC emissions are sampled simultaneously by a Tedlar bag for light HC species and by a Tenax TA™ adsorption trap for semi-volatile HC species, and they are analyzed by gas chromatography with a flame ionization detector. The bulk temperature and residence time during combustion are key parameters that are important for understanding the effects of speed and load on engine-out HC emissions. The degree of post-flame oxidation is higher in PCI than in conventional combustion, and it is increased for PCI with a higher speed and load, as indicated by a lower fuel alkanes/THC ratio, a higher alkenes/fuel alkanes ratio, and a higher methane/THC ratio. Ethene and n-undecane are two representative HC species, and they are used as a surrogate mixture in the gas flow reactor to simulate PCI and conventional combustion with in-cylinder post fuel injection. Among the three DOC formulations tested, the catalyst with constituent precious metals of platinum and palladium (PtPd) showed the best light-off performance, followed by PtPd with an addition of cerium dioxide (PtPd+CeO₂), and platinum (Pt), regardless of exhaust compositions. Conventional combustion exhaust composition shows a lower light-off temperature than that of PCI, regardless of catalyst formulation.     

燃气热泵的经济性分析

利用热经济学的研究方法对燃气热泵和其它几种常规空调方式的经济性进行了研究比较,并就能源价格变化对经济性的影响进行了研究,获得了适宜燃气热泵推广应用的能源价格范围。结果表明,燃气热泵的年度总成本最低,具有经济性优势。     

高纯六氟化钨的分析方法综述

本文介绍了六氟化钨的性质、应用及目前的发展状况,针对六氟化钨区别于其它电子气体的特殊性质,综述了对其中所含气体杂质和金属粒子的分析方法。六氟化钨中的气体杂质主要包括:四氟化碳、四氟化硅、二氧化碳、六氟化硫、氧气、氮气和一氧化碳,采用加反吹系统的气相色谱法进行分析;氟化氢杂质用傅立叶红外光谱进行分析;六氟化钨中的金属粒子主要有钙、钾、铁、铜和铬等,可以采用原子发射光谱法、原子吸收光谱法和电感耦合等离子质谱法进行测定。