原子吸收法测定钢中的铬与钼的改进

阐述了用原子吸收法测定钢中的铬、钼的方法和规程,并对影响测试结果的诸因素进行了试验和优选,使误差在国标范围之内,大大提高了分析效率,充分发挥了现代分析仪器的作用。     

分光光度计测量结果的不确定度评定

测量不确定度是对测量结果而言,表达这个结果分散性程度的参数,是计量学中的一个重要内容。本文对分光光度计校准过程的透射比示值误差测量结果的不确定度和波长示值误差测量结果的不确定度进行了评定,给出了评定方法、步骤及结果,并对测量不确定度进行了讨论。     

分析与检测

我所具有完善的质量保证体系，拥有一支经验丰富、业务精湛的检测技术人员队伍。本所拥有色谱／质量谱联用仪、色相色谱仪、高效液相色谱仪、紫外光谱仪、x-衍射仪、x-荧光仪、原子吸收光谱仪等大型进口分析仪器，可对物质的结构以及化学成分进行全面的定性、定量测定。可承担对原子吸收仪、气相色谱仪、酸度计、紫外分光光度计、电导仪等仪器的计量检定工作。     

NHT-1型不透光度计的使用与维护

NHT-1型不透光度计是用于检测压燃式柴油机排气（排烟）中可见污染物的便携式智能化仪器。它采用先进的测量技术及国外先进的测量部件，适合环境保护部门、机动车检测站、发动机制造厂、汽车制造厂、汽车修理厂等单位使用。     

THE STUDY ON THE CHANGES OF ZINC, COPPER, CALCIUM AND MAGNESIUM IN PLASMA AND ERYTHROCYTES DURING CARDIOPULMONARY BYPASS

Objective To study the changes and their influence factors involved of zinc, copper, calcium and magnesium in plasma and erythrocytes during cardiopulmonary hypass(CPB). Methods Zinc, copper, calcium and magnesium values in plasma and erythrocytes were measured by atomic absorption spectrophotometer during CPB. Results Zinc and copper levels in plasma were significantly elevated above preinduction level before perfusion, hut calcium and magnesium levels did not change significantly; zinc, copper and calcium levels in plasma were significantly below preoperation level during CPB, hut magnesium level in plasma was significantly increased above preoperation; zinc level in plasma was increased to preoperation level after CPB and began to decrease again at 8 hours after CPB,copper level in plasma was increased to preoperation level at 20 hours after CPB, calcium in plasma was increased significantly from beginning to 8 hours after CPB, magnesium level in plasma was decreased to preoperation level at 8 hours afterCPB. Concentration of zinc , copper, calcium and magnesium in erythrocytes did not change significantly. Conclusion During CPB, the changes of zinc, copper, calcium and magnesium had relation to hemodilution, operative wound, carrier protein, stress and component of priming Solution and cardioplegic solution, hut no relation to transferfrom plasma erythrocytes. The results indicate that it is beneficial to patient‘s recovery to supplement zinc, copper, calcium and magnesium properly by different ways during cardiac perioperation.     

提高原子吸收分光光度计石墨炉法测定Pb的灵敏度的研究

以20 ng/mL铅标准溶液为试样,采用HITICHI Z-2000原子吸收分光光度计石墨炉法,进行了灰化温度、原子化温度、净化温度、时间常数、灯电流、狭缝宽度和基体改进剂实验。优化确定了提高测定Pb灵敏度的实验条件,使20 ng/mL的铅标样吸光度达到厂方推荐参考值0.12以上。     

石墨炉法原子吸收温度的控制与选择对测定铅的影响

干燥温度、灰化温度、原子化温度以及净化温度的控制与保持时间选择是用好石墨炉原子吸收分光光度计关键所在。笔者通过反复实践与长期摸索，结合TAS-986原子吸收分光光度计（横向石墨管）的实际，适当改变铅测定时干燥温度、灰化温度、原子化温度以及净化温度的控制与保持时间，铅测定的准确率由87．5％提高到98．4％，效果明显。     

微机数据采集监测系统在分光光度计中的应用

对分光光度计微机数据采集监测系统的硬件、软件及网络的结构、功能，以及自行研制的小信号调理接口板和纯Delphi软件开发技术等进行了研究，成功开发出一种通用的、任意通道的微机数据采集监测系统。     

测微光度计与PC—1500数据处理系统联机应用

本文介绍了测微光度计通过SPC－3数据采集仪与PC－1500微机联机的方法和工作原理，通过联机测光有效地达到了提高测量速度和测量精确度的目的，实现了测光的半自动和数据处理的自动化，方法稳定可靠，操作简单，易于掌握。