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潜艇舱室大气中金属元素的X-射线荧光光谱法检测
引用本文:赵明,张洪彬,原霞,张海霞.潜艇舱室大气中金属元素的X-射线荧光光谱法检测[J].舰船防化,2006(Z1).
作者姓名:赵明  张洪彬  原霞  张海霞
作者单位:第七一八研究所 河北邯郸056027
摘    要:建立了X-射线荧光光谱仪对潜艇舱室大气中Cr、Mn、Fe、Co、Ni、Cu等10种金属元素的快速分析方法。利用醋酸纤维素微孔滤膜对潜艇舱室大气进行采样,用X射线荧光光谱仪对滤膜进行检测,可同时检测10种金属元素。方法具有简便准确、元素分析含量适应范围宽等优点。方法的相对标准偏差在0.99%~3.04%,回收率在94.2%~98.4%。

关 键 词:X-射线荧光光谱法  醋酸纤维素微孔滤膜  潜艇舱室大气  金属元素

Determination of Metal Elements in the Submarine Cabin Air by X-ray Fluorescence Spectrometer
Zhao Ming,Zhang Hong-bin,Yuan Xia,Zhang Hai-xia.Determination of Metal Elements in the Submarine Cabin Air by X-ray Fluorescence Spectrometer[J].Chemical Defence on Ships,2006(Z1).
Authors:Zhao Ming  Zhang Hong-bin  Yuan Xia  Zhang Hai-xia
Abstract:This paper describes a new method of the determination of 10 metal elements in the submarine cabin air by X-ray fluorescence spectrometer. Sampling the air of submarine cabin using the microporous film, determining the film with X-ray fluorescence spectrometer directly, 10 metal elements can be determined at the same time. The method is simple, fast and accurate. Its RSD is from 0.99% to 3.04%, and recovery from 94.2% to 98.4%.
Keywords:X-ray fluorescence spectrometer  Microporous film  Air in the submarine cabin  Metal elements
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